This study was carried out to evaluate the characteristics of volatile organic compounds (VOCs) and aldehydes emission as a function of airtight time in new apartment. Sampling was undertaken at 34 new apartments located in 4 different cities of Korea from February to November 2005. The measurement data were collected every one hour from 10 a.m. to 6 p.m. toward increasing airtight time in a day. The concentrations of VOCs and aldehydes were analysed by GC/MS and HPLC method, respectively. These methods showed good sensitivity, linearity, and repeatability. In this study, the most abundant compounds at new apartments appeared to be toluene, m,p-xylene, formaldehyde and acetone. Moreover, the concentration variations at a closed rooms progressively increased by airtight time of 5 hours. Airtight time of new apartment was a most important and affective factor which influenced concentration change. Keywords：Indoor air, Airtight time, New apartment, Volatile organic compounds(VOCs), Aldehydes